Xanthene → HCID 12340279, 화합물

HRID 988868

반응식

HRID 988868 반응식
[CH:1]1[C:14]2[CH2:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[O:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[Cl:15][CH2:16][CH2:17][C:18](Cl)=[O:19]>O>[Cl:15][CH2:16][CH2:17][C:18]([C:10]1[CH:9]=[CH:8][C:7]2[O:6][C:5]3[C:14](=[CH:1][C:2]([C:18](=[O:19])[CH2:17][CH2:16][Cl:15])=[CH:3][CH:4]=3)[CH2:13][C:12]=2[CH:11]=1)=[O:19]

참가 물질

4

반응물 2

HCID 7107XantheneHCID 693643-Chloropropionyl chloride

생성물 1

HCID 12340279HCID 12340279, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Prepared from xanthene 16 and 3-chloropropionyl chloride as described in Scheme 5 to give a solid. Mp 179-181° C. 1H NMR (CDCl3, 400 MHz) δ7.86-7.84 (m, 4H), 7.13 (d, J=10 Hz, 2H), 4.18 (s, 2H), 3.94 (t, J=8 Hz, 4H), 3.44 (t, J=8 Hz, 4H). Anal. (C19H16Cl2O3. 0.1 H2O).

후처리

  1. customto give a solid

출처 및 근거

ORD 기록
ord-9a4032462e6f41179b2104edec436e22
출처 데이터셋
uspto-grants-2003_10
특허 번호
US06635786B2

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