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Estradiol → Estradiol; Norethindrone Acetate

HRID 988926
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인쇄 미리보기

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HRID 988926 반응식
[CH3:1][C@@:2]12[C@@H:18]([OH:19])[CH2:17][CH2:16][C@H:15]1[C@H:14]1[C@@H:5]([C:6]3[CH:7]=[CH:8][C:9]([OH:20])=[CH:10][C:11]=3[CH2:12][CH2:13]1)[CH2:4][CH2:3]2.[CH3:21][C:22]([O:24][C@:25]1([C:44]#[CH:45])[C@@:29]2([CH3:43])[CH2:30][CH2:31][C@@H:32]3[C@@H:42]4[C:36](=[CH:37][C:38]([CH2:40][CH2:41]4)=[O:39])[CH2:35][CH2:34][C@H:33]3[C@@H:28]2[CH2:27][CH2:26]1)=[O:23].CC(O)COC(CO)C.C(O)CCCCCCC/C=C\CCCCCCCC>C(O)(C)C.C1(C)C=CC=CC=1.C(OCC)(=O)C>[CH3:1][C@@:2]12[C@@H:18]([OH:19])[CH2:17][CH2:16][C@H:15]1[C@H:14]1[C@@H:5]([C:6]3[CH:7]=[CH:8][C:9]([OH:20])=[CH:10][C:11]=3[CH2:12][CH2:13]1)[CH2:4][CH2:3]2.[CH3:21][C:22]([O:24][C@:25]1([C:44]#[CH:45])[C@@:29]2([CH3:43])[CH2:30][CH2:31][C@@H:32]3[C@@H:42]4[C:36](=[CH:37][C:38]([CH2:40][CH2:41]4)=[O:39])[CH2:35][CH2:34][C@H:33]3[C@@H:28]2[CH2:27][CH2:26]1)=[O:23]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

9

반응물 5

HCID 5757EstradiolHCID 5832Norethisterone AcetateHCID 328812-(2-Hydroxypropoxy)-1-propanolHCID 5284499Oleyl AlcoholHCID 178527255HCID 178527255, 화합물

생성물 1

HCID 3045253Estradiol; Norethindrone Acetate

시약·촉매·용매

3
HCID 1140Toluene용매HCID 3776Isopropanol용매HCID 8857Ethyl Acetate용매

실험 절차

An estradiol/norethindrone acetate pressure-sensitive adhesive matrix composition was prepared by combining 0.7 parts of estradiol and 3.0 parts of norethindrone acetate along with 3.0 parts of ethyl cellulose (Ethocele® 10, Dow Chemical Corp., Midland, Mich.) in 30.0 parts ethyl acetate, 15.0 parts of toluene and 10.0 parts isopropyl alcohol. Then 12.2 parts of a polyacrylate adhesive (DURO-TAIE® 87-2510; National Starch Company, Bridgewater, N.J.) and 109.2 parts of a polysiloxane adhesive (BIO-PSA® Q7-4603; Dow Corning Corp, Midland, Mich.) were added and thoroughly mixed. Finally 9.0 parts of dipropylene glycol and 6.0 parts oleyl alcohol were added and mixed thoroughly in an appropriate container until the mixture was completely homogenous. The resulting composition had the ingredient concentrations on a dry weight percent basis (i.e., after evaporation of volatile solvents) as shown below.

후처리

  1. additionthoroughly mixed
  2. additionmixed thoroughly in an appropriate container until the mixture
  3. concentrationthe ingredient concentrations
  4. customon a dry weight percent basis (i.e., after evaporation of volatile solvents)

출처 및 근거

ORD 기록
ord-19b297349b4b464a94791fb9bf448537
출처 데이터셋
uspto-grants-2003_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06638528B1

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