참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methyl p-toluenesulfonate | HCID 6645 | — |
| 반응물 | 2-Fluoropyridine | HCID 9746 | — |
| 생성물 | 2-Fluoro-1-methylpyridinium p-toluenesulfonate | HCID 171631 | — |
반응 단계
10 mmol of 2-fluoropyridine and 10 mmol of methyl 4-methylbenzenesulphonate are mixed in a 50 ml round-bottomed flask and stirred for 6 hours at 70° C. under a nitrogen atmosphere. The salt obtained in the form of a white solid is used without additional purification in the following step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06638946B2 |
|---|
| 출처 데이터셋 | uspto-grants-2003_10 |
|---|
| ORD ID | ord-69e889f052d14059a99a12de8bf46d29 |
|---|
| 출처 메모 | uspto-grants-2003_10 |
|---|
