참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chromium(3+) trichloride | HCID 6452300 | — |
| 반응물 | L-Ascorbic Acid | HCID 54670067 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178519210 | HCID 178519210 | — |
반응 단계
Half gram (1.85 mmole) of chromium chloride (CrCl3) was dissolved in 30 ml of deionized water to get a green solution. 1.0 g (5.5 mmole) of ascorbic acid (Asc) dissolved in 40 ml of deionized water, was added to the solution. The pH of the reaction mixture was adjusted to 4.5 (pK(Asc)4.2), and the reaction mixture was stirred for 3 hours at 50° C. to get a dark green solution. The solution was concentrated in vacuum and the large volume of ethanol 90% was added to get a green sediment. UV-VIS Spectrum for Cr-Asc showed two main absorbance peaks at 263 and 592 nm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06458351B2 |
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| 출처 데이터셋 | uspto-grants-2002_10 |
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| ORD ID | ord-41998616a7dd415388b9f444902f1e40 |
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| 출처 메모 | uspto-grants-2002_10 |
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