참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Bromo-3-chloropropane | HCID 8006 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Acetamide, N-(2-hydroxy-5-nitrophenyl)- | HCID 3292867 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | n-[2-(3-Chloropropoxy)-5-nitrophenyl]acetamide | HCID 18415451 | — |
반응 단계
A mixture of 186.5 g (0.94 mol) of N—(2-hydroxy-5-nitrophenyl)acetamide and 142.7 g (1.03 mol) of potassium carbonate in 570 ml of dimethylformamide was heated to 30-35° C. with stirring; 444.0 g (2.82 mol) of 1-bromo-3-chloropropane were then added and heating was continued at 40° C. for 7 hours (orange-coloured suspension).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06461389B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_10 |
|---|
| ORD ID | ord-1431f11f41c74938b6e443c9084a24fd |
|---|
| 출처 메모 | uspto-grants-2002_10 |
|---|
