참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | Benzoguanamine | HCID 7064 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Benzoguanamine formaldehyde | HCID 172081 | — |
반응 단계
A 4-necked flask equipped with a stirrer, a reflux condenser and a thermocouple was charged with 150 parts of benzoguanamine, 50 parts of paraformaldehyde (formaldehyde content 95%) and 120 parts of water. The pH of the mixture was adjusted to 8.5 with a 10% aqueous solution of sodium carbonate. While agitating this mixture, its temperature was raised to 90° C., and its reaction was carried out for 5 hours to obtain an aqueous liquid of a soluble and fusible benzoguanamine-formaldehyde prepolymer. The prepolymer thus obtained is cooled to 50° C. and rapidly mixed with 100 part of acetone which has also been warmed to 500° C. The product is mixed with 3.0 parts of fluorescent dye Solvent Yellow 135 at temperature 40-50° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06462128B1 |
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| 출처 데이터셋 | uspto-grants-2002_10 |
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| ORD ID | ord-0fa91092043949bd85af7eead31be5f9 |
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| 출처 메모 | uspto-grants-2002_10 |
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