4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester

HRID 991078

반응식

HRID 991078 반응식
Br[CH:2]([CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH3:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([SH:21])=[CH:17][CH:16]=1>>[CH2:6]([O:5][C:3](=[O:4])[CH:2]([S:21][C:18]1[CH:19]=[CH:20][C:15]([O:14][CH3:13])=[CH:16][CH:17]=1)[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:7]

참가 물질

3

실험 절차

2-(4-Methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (13.8 g, 98%) was prepared according to the general method as outlined in example 1 starting from ethyl 2-bromoheptanoate (11 g, 47 mmol) and 4-methoxythiophenol (6 g, 42.8 mmol), as a yellow oil; MS: 297.2 (M+H)+.

출처 및 근거

ORD 기록
ord-a24c4c085352445a978f1232c59e598c
출처 데이터셋
uspto-grants-2002_10
특허 번호
US06462073B2

연결된 노트

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