Butyryl chloride → 9H-Xanthene-9-carboxylic acid butyryl-amide

HRID 991219

반응식

[CH:1]1[C:14]2[CH:13]([C:15]([NH2:17])=[O:16])[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[O:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH2:18]([C:21](Cl)=[O:22])[CH2:19][CH3:20]>>[C:21]([NH:17][C:15]([CH:13]1[C:14]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=2[O:6][C:7]2[C:12]1=[CH:11][CH:10]=[CH:9][CH:8]=2)=[O:16])(=[O:22])[CH2:18][CH2:19][CH3:20]

참가 물질

반응물 2

HCID 8855Butyryl chloride

HCID 7255769H-Xanthene-9-carboxamide

생성물 1

HCID 542148309H-Xanthene-9-carboxylic acid butyryl-amide

실험 절차

The title compound, white solid, m.p. 222° C. and MS: m/e=295 (M+) was prepared in accordance with the general method of example 39 from 9H-xanthene-9-carboxylic acid amide and propanecarboxylic acid chloride.

출처 및 근거

ORD 기록: ord-dea92825a38b4fd1938706eb996e2897
출처 데이터셋: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06462198B1

연결된 노트

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