2,2-Diphenylacetyl chloride → N-(3-Methyl-[1,2,4]oxadiazol-5-yl)-2,2-diphenyl-acetamide

HRID 991246

반응식

HRID 991246 반응식
[CH3:1][C:2]1[N:6]=[C:5]([NH2:7])[O:4][N:3]=1.[C:8]1([CH:14]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:15](Cl)=[O:16])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[CH3:1][C:2]1[N:6]=[C:5]([NH:7][C:15](=[O:16])[CH:14]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[O:4][N:3]=1

참가 물질

3

반응물 2

HCID 746372,2-Diphenylacetyl chlorideHCID 5671183-Methyl-1,2,4-oxadiazol-5-amine

생성물 1

HCID 9839036N-(3-Methyl-[1,2,4]oxadiazol-5-yl)-2,2-diphenyl-acetamide

실험 절차

The title compound, white solid, m.p. 215° C. and MS: m/e=293 (M+) was prepared in accordance with the general method of example 44a from 3-methyl-[1,2,4]oxadiazol-5-ylamine (Helv. Chim. Acta, 49(1966), 1430-1432) and 2,2-diphenylacetic acid chloride.

출처 및 근거

ORD 기록
ord-f353b7d105ba420ebd86808902294df0
출처 데이터셋
uspto-grants-2002_10
특허 번호
US06462198B1

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