Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Iminoethyl methoxyacetate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Methoxyacetonitrile | HCID 74442 | — |
| 생성물 | Iminoethyl methoxyacetate hydrochloride | HCID 57478929 | — |
반응 단계
A solution of 35.5 g (0.50 mol) of methoxyacetonitrile in 29 ml (23 g, 0.50 mol) of ethanol and 30 ml of absolute diethylether was cooled to 0° C. and over 1 hour 22.5 g (0.62 mol) of hydrogen chloride gas was introduced, whilst towards the end of the introduction of gas the reaction product crystallised out. To complete the precipitation 130 ml of diethylether were added and the colourless needles were filtered off.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06469039B1 |
| 출처 데이터셋 | uspto-grants-2002_10 |
| ORD ID | ord-a52066071dfd4d80a5ea89aab03b1819 |
| 출처 메모 | uspto-grants-2002_10 |