4-(1H-Pyrazol-1-yl)benzaldehyde → 3-[4-(4-Methyl-2-pyrimidinyl)phenyl]-2-propenal

반응식

[CH3:1][C:2]1[CH:7]=[CH:6][N:5]=[C:4]([C:8]2[CH:15]=[CH:14][C:11]([CH:12]=O)=[CH:10][CH:9]=2)[N:3]=1.N1(C2C=C[C:24]([CH:25]=[O:26])=CC=2)C=CC=N1>>[CH3:1][C:2]1[CH:7]=[CH:6][N:5]=[C:4]([C:8]2[CH:15]=[CH:14][C:11]([CH:12]=[CH:24][CH:25]=[O:26])=[CH:10][CH:9]=2)[N:3]=1

참가 물질

반응물 2

HCID 27764774-(1H-Pyrazol-1-yl)benzaldehyde

HCID 226308614-(4-Methylpyrimidin-2-YL)benzaldehyde

생성물 1

HCID 739903413-[4-(4-Methyl-2-pyrimidinyl)phenyl]-2-propenal

실험 절차

The title compound was prepared by a procedure analogous to Reference Example 30 by substituting 4-(4-methyl-2-pyrimidinyl)benzaldehyde (prepared as described in Reference Example 14) for the 4-(1H-pyrazol-1-yl)-benzaldehyde of Reference Example 30. MS 225 (M+H)+.

출처 및 근거

ORD 기록: ord-28ea3d41b1dc4e3cbd6eb07498e86d2f
출처 데이터셋: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06472372B1

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