Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-5-nitrobenzenesulfonic acid → 2-Carboxy-nitrobenzenesulfonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-5-nitrobenzenesulfonic acid | HCID 8458 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Potassium Permanganate | HCID 516875 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Carboxy-nitrobenzenesulfonic acid | HCID 19693800 | — |
반응 단계
400.0 g (2.53 mol) of potassium permanganate are added in portions at 80° C. over a period of 2 h to a solution of 106.0 g (0.40 mol) of 2-methyl-5-nitrobenzenesulfonic acid and 80.0 g (0.58 mol) of potassium carbonate in 1300 ml of water. The reaction temperature is maintained at between 80° and 95° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723409 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-b384396be0494ddab64c768366b631a5 |
| 출처 메모 | uspto-grants-1998_03 |