HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → 2-Methyl-1-naphthalenol propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | 1-Naphthol | HCID 7005 | — |
| Reactant | 2-Methyl-1-naphthol | HCID 24055 | — |
| Reactant | Acetic acid, 2,2,2-trifluoro-, phenyl ester | HCID 68143 | — |
| Reactant | 2-Methyl-1-naphthalenol methylcarbonate | HCID 18795220 | — |
| Product | 2-Methyl-1-naphthalenol propionate | HCID 15394711 | — |
Reaction Steps
To demonstrate the storage stability of the compounds of the present invention, test samples of the title compounds of Examples 1, 2, 3, 4, 5 and 6 were placed in clear glass vials and kept on top of a laboratory desk for the time indicated. Samples of 2-methyl-1-naphthol, 1-naphthol and phenyl trifluoroacetate used as controls were similarly kept. One sample of 2-methyl-1-naphthol was stored under nitrogen and in a dry ice chest (temperature of approximately -50° C). A second sample of 2-methyl-1-naphthol and the remaining test'samples were stored at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06045590 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-72b9389a07ab4ed7a519daf6acf82b59 |
| Source note | uspto-grants-2000_04 |