2-Amino-4,6-dimethylpyridine → HCID 178475872, compound

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Reaction Steps

The method of preparation of 2-Imino-3-methylpiperidine acetate, EXAMPLE 6, was used to convert 2-amino-4,6-dimethylpyridine to the title compound which was obtained as a white solid. The analysis of the product was found to be consistent with the proposed structure. m.p. 163-166° C. MH+=127; 1H NMR (D2O): δ3.48-3.40 (m, 1H); 2.52-2.40 (m, 1H); 2.07-1.95 (m, 1H); 1.85-1.75 (m, 2H); 1.75 (s, 3H); 1.12 (d, J=6.3 Hz, 3H); 1.02-0.92 (m, 1H); 0.86 (d, J=6.3 Hz, 3H).

Provenance & Evidence