Ammonium Chloride → HCID 178425252, compound

HRID 1003428Notes

Reaction equation

HRID 1003428 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][C:7]([CH3:11])([CH3:10])[CH2:8][N:9]=1.[Cl-:12].[NH4+:13]>CO>[ClH:12].[CH3:10][C:7]1([CH3:11])[CH2:8][NH:9][C:3](=[NH:13])[CH2:4][CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428605HCID 18428605, compound

Product 1

HCID 178425252HCID 178425252, compoundYield 91.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 63 (490 mg, 3.2 mmol) in 18 mL of MeOH was reacted with ammonium chloride (125 mg, 2.4 mmol) by the method of EXAMPLE 27 to yield 387 mg (69%) of the title material.

Sources & evidence

ORD record
ord-c70fb6b94bb84f1182f98e9e8fd867fa
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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