Ammonium Chloride → HCID 178440909, compound

HRID 1003433Notes

Reaction equation

HRID 1003433 reaction equation
[CH3:1][C:2]([CH:5]1[C:11](OC)=[N:10][CH2:9][CH2:8][CH2:7][CH2:6]1)([CH3:4])[CH3:3].[Cl-:14].[NH4+:15]>CO>[ClH:14].[CH3:1][C:2]([CH:5]1[CH2:6][CH2:7][CH2:8][CH2:9][NH:10][C:11]1=[NH:15])([CH3:4])[CH3:3]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428484HCID 18428484, compound

Product 1

HCID 178440909HCID 178440909, compoundYield 63.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 99 (551 mg, 2.7 mmol) in 10 mL of MeOH was reacted with ammonium chloride (145 mg, 2.7 mmol) by the method of EXAMPLE 27 to yield 350 mg of the crude title material.

Sources & evidence

ORD record
ord-e9bcdc27b5f54e46ab63919fe4225c63
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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