Ammonium Chloride → HCID 178440870, compound
Reaction equation
[CH3:1][C:2]([CH:5]1[CH2:11][CH2:10][CH2:9][CH2:8][C:7](OC)=[N:6]1)([CH3:4])[CH3:3].[Cl-:14].[NH4+:15]>CCO>[ClH:14].[CH3:1][C:2]([CH:5]1[NH:6][C:7](=[NH:15])[CH2:8][CH2:9][CH2:10][CH2:11]1)([CH3:4])[CH3:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The product of EXAMPLE 100 (174 mg, 1.0 mmol) in 10 mL of EtOH was reacted with ammonium chloride (51 mg, 1.0 mmol) by the method of EXAMPLE 27 to yield the crude title material.
Sources & evidence
- ORD record
- ord-02da1bd10eaa4b4d87a487f36a28ab11
- Source dataset
- uspto-grants-2000_04
- Patent number
- US06046211
Reaction notes
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