Ammonium Chloride → HCID 178439140, compound

HRID 1003435Notes

Reaction equation

HRID 1003435 reaction equation
CO[C:3]1[CH:4]([CH2:10][CH:11]=[CH2:12])[CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:4]1[CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:3]1=[NH:14])[CH:11]=[CH2:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 10607182HCID 10607182, compound

Product 1

HCID 178439140HCID 178439140, compoundYield 78.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 105 (90 mg, 0.54 mmol) in 10 mL of MeOH was reacted with ammonium chloride (24.5 mg, 0.46 mmol) by the method of EXAMPLE 27 to yield 68 mg (67%) of the title material.

Sources & evidence

ORD record
ord-2dc8ba4f1b1741e0b7825553938c1ebe
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

Loading…