Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 18428508, compound

HRID 1003470Notes

Reaction equation

HRID 1003470 reaction equation
[O:1]=[C:2]1[NH:8][CH:7]([CH2:9][CH2:10][CH2:11][CH:12]([NH:18][C:19]([O:21][CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[O:20])[C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH2:6][CH2:5][CH2:4][CH2:3]1.F[B-](F)(F)F.[CH3:34][O+](C)C>C(Cl)Cl>[CH3:34][O:1][C:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]([CH2:9][CH2:10][CH2:11][CH:12]([NH:18][C:19]([O:21][CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[O:20])[C:13]([O:15][CH2:16][CH3:17])=[O:14])[N:8]=1

Participants

4

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 18428458HCID 18428458, compound

Product 1

HCID 18428508HCID 18428508, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The product of EXAMPLE 247 is treated with trimethyloxonium tetraflouroborate in CH2Cl2 by the method of EXAMPLE 26 to yield title material.

Workup

  1. customto yield title material

Sources & evidence

ORD record
ord-85b9bbf57f384e4db4a1a916e986f1e9
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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