Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → 3,4-dihydro-5-methoxy-3-methyl-2-(2-propenyl)-2H-pyrrole
Reaction equation
[CH3:1][CH:2]1[CH:6]([CH2:7][CH:8]=[CH2:9])[NH:5][C:4](=[O:10])[CH2:3]1.F[B-](F)(F)F.[CH3:16][O+](C)C>>[CH3:16][O:10][C:4]1[CH2:3][CH:2]([CH3:1])[CH:6]([CH2:7][CH:8]=[CH2:9])[N:5]=1Participants
3
Procedure
The product of EXAMPLE 265 is reacted with trimethyloxonium tetrafluoroborate by the method of EXAMPLE 26 to produce the title material.
Sources & evidence
- ORD record
- ord-f089ecb92ce3412c9cff6bafa58efd20
- Source dataset
- uspto-grants-2000_04
- Patent number
- US06046211
Reaction notes
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