Ammonium Chloride → HCID 178478662, compound

HRID 1003482Notes

Reaction equation

HRID 1003482 reaction equation
[O:1]=[C:2]1[O:6][CH:5]([CH:7]([NH:20]C(=O)OC(C)(C)C)[CH2:8][CH2:9][CH2:10][CH:11]2[CH2:17][CH2:16][CH2:15][CH2:14][C:13](OC)=[N:12]2)[CH2:4][O:3]1.[Cl-:28].[NH4+:29].Cl.CCOC(C)=O>CO>[ClH:28].[ClH:28].[NH2:20][CH:7]([CH:5]1[CH2:4][O:3][C:2](=[O:1])[O:6]1)[CH2:8][CH2:9][CH2:10][CH:11]1[CH2:17][CH2:16][CH2:15][CH2:14][C:13](=[NH:29])[NH:12]1

Participants

5

Reactant 3

HCID 25517Ammonium ChlorideHCID 18428430HCID 18428430, compoundHCID 21866389Hydrogen chloride-ethyl acetate

Product 1

HCID 178478662HCID 178478662, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 271 in MeOH is reacted with ammonium chloride by the method of EXAMPLE 27. This product is then treated with 3M HCl/EtOAc to generate the title material.

Sources & evidence

ORD record
ord-59f67a729fe543038f8edc79984b63cb
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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