Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 54379138, compound

HRID 1003500Notes

Reaction equation

HRID 1003500 reaction equation
[CH:1]([CH:5]1[NH:11][C:10](=[O:12])[CH2:9][CH2:8][CH2:7][CH2:6]1)=[CH:2][CH2:3][CH3:4].F[B-](F)(F)F.[CH3:18][O+](C)C>>[CH3:18][O:12][C:10]1[CH2:9][CH2:8][CH2:7][CH2:6][CH:5]([CH:1]=[CH:2][CH2:3][CH3:4])[N:11]=1

Participants

3

Reactant 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 54203828HCID 54203828, compound

Product 1

HCID 54379138HCID 54379138, compoundYield 103.4%

Procedure

The product of Example 326 (1.34 g, 8 mmol) was reacted with trimethyloxonium tetrafluoroborate (1.63 g, 11 mmol) by the method of Example 26 to yield 1.5 g (100%) of the title material.

Sources & evidence

ORD record
ord-3c8040e965ee470a907dd499b6e7afd8
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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