HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloroindole → 5-chloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloroindole | HCID 87110 | — |
| Reactant | Piperonylamine | HCID 2723901 | — |
| Product | 5-chloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 3050532 | 31.2% |
Reaction Steps
Beginning with 3.0 gm (20.0 mMol) 5-chloro-1H-indole and 6.0 gm (40.0 mMol) 4-piperidone hydrochloride monohydrate, 1.45 gm (31%) of the title compound were recovered as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046215 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-51865d79e5dd4425868b678d29a9819a |
| Source note | uspto-grants-2000_04 |