HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromoindole → 5-Bromo-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromoindole | HCID 24905 | — |
| Reactant | Piperonylamine | HCID 2723901 | — |
| Product | 5-Bromo-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 2763724 | 93.5% |
Reaction Steps
Beginning with 6.2 gm (31.6 mMol) 5-bromo-1H-indole and 4.7 gm (30.6 mmol) 4-piperidone monohydrate hydrochloride, 7.93 gm (93%) of the title compound were recovered as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046215 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-c8a77bec938c43eb84344ad49febd5ab |
| Source note | uspto-grants-2000_04 |