HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21268219, compound → HCID 21268220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21268219 | HCID 21268219 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21268220 | HCID 21268220 | 88.7% |
Reaction Steps
A solution of 0.29 gm (0.79 mMol) 4-chloro-2-(4-hydroxy-1-(tert-butoxycarbonyl)piperidin-4-yl)benzothiophene in 4.0 mL dichloromethane was subjected to the reaction conditions described in Example 51, providing 0.175 gm (88%) of 4-chloro-2-(1,2,3,6-tetrahydropyridin-4-yl)benzothiophene as a tan powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046215 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-eaa454ae9754412d9954b13cb643b8f0 |
| Source note | uspto-grants-2000_04 |