HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21866069, compound → HCID 21268229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21866069 | HCID 21866069 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21268229 | HCID 21268229 | 90.5% |
Reaction Steps
A solution of 1.04 gm (2.83 mMol) 6-chloro-2-(4-hydroxy-1-(tert-butoxycarbonyl)piperidin-4-yl)benzothiophene in 30.0 mL dichloromethane was subjected to the reaction conditions described in Example 51, providing 0.64 gm (90%) of 6-chloro-2-(1,2,3,6-tetrahydropyridin-4-yl)benzothiophene as a tan powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046215 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-8c3d82f2e3114a7aa14846d8516f788f |
| Source note | uspto-grants-2000_04 |