HRID1003649

反应详情

EQUATION

反应方程式

HRID 1003649 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

L-Cysteine hydrochloride monohydrate (2.0 g) is dissolved in a 2 N aqueous sodium hydroxide solution (11.4 ml). To the solution is added a solution of α-bromo-p-xylene (2.3 g) in ethanol (10 ml). The mixture is stirred at room temperature for 40 minutes, and precipitating crystals are filtered off. The obtained crystals are purified by recrystallization to give the titled compound.

WORKUP

后处理

  1. customprecipitating crystals
  2. filtrationare filtered off
  3. customThe obtained crystals are purified by recrystallization