Cyclohexylhydroxylamine → HCID 85054662, compound

HRID 1003659Notes

Reaction equation

HRID 1003659 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH:7]=O)[CH3:2].[CH:14]1([NH:20][OH:21])[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:20]([CH:14]2[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]2)[O-:21])[CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH3:2]

Participants

3

Reactant 2

HCID 72935CyclohexylhydroxylamineHCID 2447283-Ethoxy-4-methoxybenzaldehyde

Product 1

HCID 85054662HCID 85054662, compound

Procedure

The title compound was prepared according to the procedure described in Example 11 using 3-ethoxy-4-methoxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was isolated in 57% yield as a solid, m.p. 113.5° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-4ec3eaddd26e4175a118d1a4bf919fc1
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

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