Cyclohexylhydroxylamine → alpha-(3,4Ethylenedioxyphenyl)-N-cyclohexylnitrone

HRID 1003660Notes

Reaction equation

HRID 1003660 reaction equation
[CH2:1]1[CH2:12][O:11][C:10]2[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][C:3]=2[O:2]1.[CH:13]1([NH:19][OH:20])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH2:1]1[CH2:12][O:11][C:10]2[CH:9]=[CH:8][C:5]([CH:6]=[N+:19]([CH:13]3[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]3)[O-:20])=[CH:4][C:3]=2[O:2]1

Participants

3

Reactant 2

HCID 72935CyclohexylhydroxylamineHCID 2481272,3-Dihydro-1,4-benzodioxin-6-carbaldehyde

Product 1

HCID 85049697alpha-(3,4Ethylenedioxyphenyl)-N-cyclohexylnitrone

Procedure

The title compound was prepared according to the procedure described in Example 11 using 3,4ethylenedioxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was isolated in 74.5% yield as a solid, m.p. 96.7° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-43083891f30e4e6c905b594687e2a20b
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

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