Benzaldehyde, 2-ethoxy- → HCID 85044747, compound

HRID 1003663Notes

Reaction equation

[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)[CH3:2].[CH:12]([NH:15][OH:16])([CH3:14])[CH3:13]>>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=[N+:15]([CH:12]([CH3:14])[CH3:13])[O-:16])[CH3:2]

Participants

Reactant 2

HCID 11950Benzaldehyde, 2-ethoxy-

HCID 78763Isopropylhydroxylamine

Product 1

HCID 85044747HCID 85044747, compound

Procedure

The title compound was prepared according to the procedure described in Example 11 using 2-ethoxybenzaldehyde and N-isopropylhydroxylamine. The title compound was isolated in 48.8% yield as a solid, m.p. 59.4° C. (Rf =0.48 on a silica gel plate using ethyl acetate as the eluant).

Workup

customThe title compound was prepared

Sources & evidence

ORD record: ord-846072823ca34f178a6b2f156873c755
Source dataset: uspto-grants-2000_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06046232

Reaction notes

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