Benzaldehyde, 2-ethoxy- → alpha-(Ethoxyphenyl)-N-cyclohexylnitrone

HRID 1003664Notes

Reaction equation

HRID 1003664 reaction equation
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)[CH3:2].[CH:12]1([NH:18][OH:19])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1>>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=[N+:18]([CH:12]1[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1)[O-:19])[CH3:2]

Participants

3

Reactant 2

HCID 11950Benzaldehyde, 2-ethoxy-HCID 72935Cyclohexylhydroxylamine

Product 1

HCID 86587895alpha-(Ethoxyphenyl)-N-cyclohexylnitrone

Procedure

The title compound was prepared according to the procedure described in Example 11 using 2-ethoxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was isolated in 89% yield as a solid, m.p. 54.8° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-bec2f24f83624a15b3432cfbac03b842
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

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