Ethylvanillin → HCID 86587900, compound

HRID 1003670Notes

Reaction equation

[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[OH:12])[CH:7]=O)[CH3:2].I[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH:20]([NH:23][OH:24])([CH3:22])[CH3:21]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:23]([CH:20]([CH3:22])[CH3:21])[O-:24])[CH:9]=[CH:10][C:11]=1[O:12][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH3:2]

Participants

Reactant 3

HCID 8467Ethylvanillin

HCID 125271-Iodohexane

HCID 78763Isopropylhydroxylamine

Product 1

HCID 86587900HCID 86587900, compound

Procedure

The title compound was prepared according to the procedure described in Example 28 using 3-ethoxy-4-hydroxybenzaldehyde, 1-iodohexane and N-isopropylhydroxylamine. The title compound was isolated in 47.1 % overall yield as a solid, m.p. 69.0° C.

Workup

customThe title compound was prepared

Sources & evidence

ORD record: ord-21c5e5fca35d4ac9927eadd4d4d90816
Source dataset: uspto-grants-2000_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06046232

Reaction notes

Loading…