3,4-Diethoxybenzaldehyde → HCID 86587904, compound

HRID 1003674Notes

Reaction equation

HRID 1003674 reaction equation
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH2:13][CH3:14])[CH:7]=O)[CH3:2].[C:15]([NH:19][OH:20])([CH3:18])([CH3:17])[CH3:16]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:19]([C:15]([CH3:18])([CH3:17])[CH3:16])[O-:20])[CH:9]=[CH:10][C:11]=1[O:12][CH2:13][CH3:14])[CH3:2]

Participants

3

Reactant 2

HCID 748473,4-DiethoxybenzaldehydeHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 86587904HCID 86587904, compound

Procedure

The title compound was prepared according to the procedure described in Example 11 using 3,4-diethoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 93.7% yield as a solid, m.p. 57.9° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-b515ec441c1447608c26318fb2f5a916
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

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