HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodoheptane → HCID 86587905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodoheptane | HCID 20274 | — |
| Reactant | N-tert-butylhydroxylamine | HCID 98586 | — |
| Reactant | 2-Fluoro-4-hydroxybenzonitrile | HCID 2734675 | — |
| Product | HCID 86587905 | HCID 86587905 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 28 using 2-fluoro-4-hydroxybenzonitrile, 1-iodoheptane and N-tert-butylhydroxylamine. The title compound was isolated in 66.0% overall yield as a white solid, m.p. 38.8° C. (Rf =0.21 on a silica gel plate using hexanes/ethyl acetate, 4:1, v:v, as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046232 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-be6dd470476b46c7917c60781f0c354f |
| Source note | uspto-grants-2000_04 |