HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 86587907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Cyclohexylhydroxylamine | HCID 72935 | — |
| Reactant | 2-Fluoro-4-hydroxybenzonitrile | HCID 2734675 | — |
| Product | HCID 86587907 | HCID 86587907 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 29 using 2-fluoro-4-hydroxybenzonitrile, ethyl iodide and N-cyclohexylhydroxylamine. The title compound was isolated in 58.8% overall yield as slightly yellowish crystals, m.p. 112.7° C. (Rf =0.17 on a silica gel plate using hexanes/ethyl acetate, 4:1, v:v, as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046232 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-81174546d7de4004807618f3dec747b6 |
| Source note | uspto-grants-2000_04 |