HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Hydroxyphenyl)-1-phenylprop-2-en-1-one → NSC179363
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Hydroxyphenyl)-1-phenylprop-2-en-1-one | HCID 89340 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | NSC179363 | HCID 301514 | — |
Reaction Steps
The title compound was prepared as described in General Method 3 from 3-(4-hydroxy-phenyl)-1-phenyl-prop-2-en-1-one (25.5 g, 113.6 mmol), 5% Pd on BaSO4 (1.0 g), and THF (400 mL). The catalyst was filtered, and the filtrate was concentrated. The residue was recrystallized from 50% EtOH, to give the title compound, m.p. 118-119° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046355 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-477822dfe3164ba086aaeb4f30bcb4d6 |
| Source note | uspto-grants-2000_04 |