Chloroform → HCID 12571729, compound

HRID 1003967Notes

Reaction equation

HRID 1003967 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][C:11]([OH:13])=[O:12])=[CH:6][CH:5]=1)([CH3:3])[CH3:2].[CH:14](Cl)(Cl)Cl>>[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][C:11]([O:13][CH3:14])=[O:12])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]

Participants

3

Procedure

Prepared from 4-isopropylphenylacetic acid (Lancaster) by the method described in Example 34a). νmax (CHCl3)/cm-1 1735. δH (250 MHz, CDCl3), 1.24 (6H, d, J 6.96), 2.90 (1H, heptet, J 6.93), 3.60 (2H, s), 3.69 (3H, s), 7.16-7.24 (5H, m).

Sources & evidence

ORD record
ord-95170512fece44c0b357a2342c5f078d
Source dataset
uspto-grants-2000_04
Patent number
US06048852

Reaction notes

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