4-Bromo-2,6-dimethylbenzaldehyde → 2,6-Dimethyl4-isopropylbenzyl alcohol

HRID 1003979Notes

Reaction equation

HRID 1003979 reaction equation
Br[C:2]1[CH:9]=[C:8]([CH3:10])[C:5]([CH2:6][OH:7])=[C:4]([CH3:11])[CH:3]=1.Br[C:13]1[CH:20]=C(C)C(C=O)=C(C)[CH:14]=1>>[CH3:10][C:8]1[CH:9]=[C:2]([CH:13]([CH3:20])[CH3:14])[CH:3]=[C:4]([CH3:11])[C:5]=1[CH2:6][OH:7]

Participants

3

Reactant 2

HCID 110202224-Bromo-2,6-dimethylbenzaldehydeHCID 14680145(4-Bromo-2,6-dimethylphenyl)methanol

Product 1

HCID 154807012,6-Dimethyl4-isopropylbenzyl alcoholYield 95%

Procedure

4-Bromo-2,6-di methylbenzyl alcohol, from 4-bromo-2,6-dimethylbenzaldehyde (Hjed, H. et al. Acta Chem. Scand. 1965, 19:2166); 95% yield, mp 1 17-119° C.

Workup

  1. custom95% yield, mp 1 17-119° C.

Sources & evidence

ORD record
ord-a454f6abac024e96823f2436882ad9ea
Source dataset
uspto-grants-2000_04
Patent number
US06048862

Reaction notes

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