HCID 86755305, compound → HCID 9892625, compound
Reaction equation
[CH3:1][O:2][C:3]1[C:35]([O:36][CH3:37])=[CH:34][C:6]2[S:7][C:8](/[CH:23]=[C:24](\[C:28]3[CH:33]=[CH:32]N=[CH:30][CH:29]=3)/[C:25]([O-:27])=[O:26])=[C:9]([O:10][C:11]3[CH:20]=[CH:19][C:18]4[C:13](=[CH:14][CH:15]=[C:16]([O:21][CH3:22])[CH:17]=4)[CH:12]=3)[C:5]=2[CH:4]=1.[Na+].[CH3:39]OC1C(OC)=CC2SC(/C=C(\C3C=CC=CC=3)/C([O-])=O)=C(OC3C=CC(OC)=CC=3)C=2C=1.[Na+]>>[CH3:1][O:2][C:3]1[C:35]([O:36][CH3:37])=[CH:34][C:6]2[S:7][C:8](/[CH:23]=[C:24](\[C:28]3[CH:33]=[CH:32][CH:39]=[CH:30][CH:29]=3)/[C:25]([OH:27])=[O:26])=[C:9]([O:10][C:11]3[CH:20]=[CH:19][C:18]4[C:13](=[CH:14][CH:15]=[C:16]([O:21][CH3:22])[CH:17]=4)[CH:12]=3)[C:5]=2[CH:4]=1Participants
3
Procedure
The procedure is as for Example 1 using the reagent of Example 5 in Step E, and the reagent of Example 6 in Step F.
Sources & evidence
- ORD record
- ord-e4bafa0167204f2a8b29d454b9295182
- Source dataset
- uspto-grants-2000_04
- Patent number
- US06048875
Reaction notes
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