HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23434143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 12112779 | HCID 12112779 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | HCID 23434143 | HCID 23434143 | 70.2% |
Reaction Steps
A mixture of 3-cyano-2,5-di(4-pyridyl)thiophene (40 mg, 0.152 mmol), potassium hydroxide (25 mg, 0.446 mmol) in 2-methyl-2-propanol (2 mL) was heated at reflux temperature for 2 hours. After cooling, the mixture was poured into water. The precipitates were collected by filtration, and dried under reduced pressure to give the title compound (30 mg, 70% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048880 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-9d2fc2310717420d93a603f053092681 |
| Source note | uspto-grants-2000_04 |