Ammonia → HCID 22678242, compound

Participants

Reaction Steps

A solution of 26-4 (0.19 g, 0.67 mmol) in THF (5 mL) was cooled to 0° and saturated with NH3 gas. The mixture was stirred at 0° for 4 h, then evaporated and the residue partitioned between EtOAc and sat. NaHCO3. The organic layer was dried filtered and concentrated to give the amino ester 26-5.

Provenance & Evidence