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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1004298Generated: October 31, 2026

HCID 54255487, compound → HCID 54252689, compound

https://huagongshe.com/reaction/1004298

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54255487HCID 54255487—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 54252689HCID 54252689—

Reaction Steps

To a stirred suspension of 10% palladium on carbon (15 mg) in ethanol (2 mL) was added a solution of 3-phenyl-9-(5,6,7,8-tetrahydro-[1,8]naphthyridin-2-yl)-non-2-enoic acid tert-butyl ester 29-7a (62 mg) in ethanol (3 mL) and the mixture was subjected to an atmosphere of hydrogen for 6 hours. The reaction mixture was filtered through Celite and concentrated at reduced pressure to give 29-8a as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06048861
Source datasetuspto-grants-2000_04
ORD IDord-bafdf25a5313465c98569baa99f8889f
Source noteuspto-grants-2000_04