Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Triethoxysilane | HCID 13830 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Phenethyltriethoxysilane | HCID 11097560 | 1.5% |
Reaction Steps
130 mg Of styrene and 217 mg of triethoxysilane were placed in a glass reaction tube and 0.01 ml of an isopropyl alcohol solution of chloroplatinic acid (platinum content: 0.02 Wt. %) was added to this mixture. The reaction tube was sealed with Teflon tape and heated for 30 minutes in an oil bath at 50° C. When the tube contents were analyzed by GC-MS following cooling, the conversion rate of styrene was 3% and phenethyltriethoxysilane was produced at a yield of 1.5%. The yield of (α-methylbenzyl) triethoxysilane was 0.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06048994 |
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| Source dataset | uspto-grants-2000_04 |
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| ORD ID | ord-fac2ab9c772f4f80b67556960349fc31 |
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| Source note | uspto-grants-2000_04 |
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