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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1004512Generated: October 30, 2026

Water → HCID 23371390, compound

https://huagongshe.com/reaction/1004512

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantPotassium CarbonateHCID 11430—
Reactant4-CyanophenolHCID 13019—
ReactantEthyl 4-bromobutyrateHCID 76300—
SolventDimethylformamideHCID 6228—
ProductHCID 23371390HCID 23371390—

Reaction Steps

4-Cyanophenol (5.0 g) is dissolved in DMF (6 ml), and thereto are added ethyl 4-bromobutanate (7.94 ml) and potassium carbonate (6.4 g), and the mixture is stirred at room temperature for 74 hours. The reaction mixture is poured into water, and the colorless precipitates are collected by filtration and washed with water to give the title compound (9.5 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06048854
Source datasetuspto-grants-2000_04
ORD IDord-90e85b85b2c745f6adbb349ace91e54e
Source noteuspto-grants-2000_04