HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23371390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Ethyl 4-bromobutyrate | HCID 76300 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23371390 | HCID 23371390 | — |
Reaction Steps
4-Cyanophenol (5.0 g) is dissolved in DMF (6 ml), and thereto are added ethyl 4-bromobutanate (7.94 ml) and potassium carbonate (6.4 g), and the mixture is stirred at room temperature for 74 hours. The reaction mixture is poured into water, and the colorless precipitates are collected by filtration and washed with water to give the title compound (9.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048854 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-90e85b85b2c745f6adbb349ace91e54e |
| Source note | uspto-grants-2000_04 |