HCID 86755332, compound → HCID 86755331, compound

Participants

Reaction Steps

1.7 g (5.8 mmol) of cis-(±)-1-benzyl-8-methoxy-2,3,3a,4,9,9a-hexahydro-1H-benz[f]indole (9b) are dissolved in 35 mL of methanol and hydrogenated at 20° C. and 5 bars of hydrogen pressure on 0.2 g of Pd/C (10%). After 5 h the mixture is filtered over silica gel and the solvent is eliminated in vacuo. 1.2 g (100%) 10b are obtained as an oil.

Provenance & Evidence