HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 18790893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 18790896 | HCID 18790896 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18790893 | HCID 18790893 | 72.8% |
Reaction Steps
A dichloromethane (1 ml) solution of 6-butyloct-7-en-1-ol (400 mg, 2.17 mmol ) was oxidized with a suspension of pyridinium chlorochromate (0.65 g, 3 mmol) and sodium acetate (20 mg) in 2 ml of dichloromethane. Standard work-up followed by PMLPC yielded 288 mg (70%) of 6-butyloct-7-enaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054141 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-d0fb67af21984152a567152e77f371f0 |
| Source note | uspto-grants-2000_04 |