Methylhydrazine → HCID 67650124, compound

HRID 1005284Notes

Reaction equation

HRID 1005284 reaction equation
[CH3:1][NH:2][NH2:3].[Cl:4][C:5]1[CH:12]=[C:11]([Cl:13])[CH:10]=[CH:9][C:6]=1[CH:7]=O>C(O)C>[CH3:1][NH:2][N:3]=[CH:7][C:6]1[CH:9]=[CH:10][C:11]([Cl:13])=[CH:12][C:5]=1[Cl:4]

Participants

4

Reactant 2

HCID 6061MethylhydrazineHCID 134042,4-Dichlorobenzaldehyde

Product 1

HCID 67650124HCID 67650124, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

263 g (5.7 mol) of methylhydrazine were treated with a solution of 200 g (1.14 mol) of 2,4-dichlorobenzaldehyde in 1.2 l of ethanol. After the mixture had been stirred for 48 hours, the small amount of solids present was filtered off and the filtrate was then concentrated. Yield: quantitative.

Workup

  1. filtrationthe small amount of solids present was filtered off
  2. concentrationthe filtrate was then concentrated

Sources & evidence

ORD record
ord-88b4be9bcc7f4915b2b2555cff7fa137
Source dataset
uspto-grants-2000_04
Patent number
US06054412

Reaction notes

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