Sulfuryl chloride → HCID 18791033, compound

HRID 1005288Notes

Reaction equation

HRID 1005288 reaction equation
[Cl:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([C:9]2[CH:13]=[C:12]([CH3:14])[N:11]([S:15]([CH3:18])(=[O:17])=[O:16])[N:10]=2)=[C:4]([F:19])[CH:3]=1.S(Cl)([Cl:23])(=O)=O>C(Cl)(Cl)(Cl)Cl>[Cl:23][C:13]1[C:9]([C:5]2[CH:6]=[C:7]([CH3:8])[C:2]([Cl:1])=[CH:3][C:4]=2[F:19])=[N:10][N:11]([S:15]([CH3:18])(=[O:17])=[O:16])[C:12]=1[CH3:14]

Participants

4

Reactant 2

HCID 24648Sulfuryl chlorideHCID 18791028HCID 18791028, compound

Product 1

HCID 18791033HCID 18791033, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

0.8 g (2.7 mmol) of 3-(4-chloro-2-fluoro-5-methylphenyl)-5-methyl-1-methylsulfonyl-1H-pyrazole and 0.4 g (3.0 mmol) of sulfuryl chloride were reacted in 50 ml of carbon tetrachloride by the method of Example 2. Yield: 0.1 g.

Sources & evidence

ORD record
ord-a4e79635fbeb47e681076c2535feb343
Source dataset
uspto-grants-2000_04
Patent number
US06054413

Reaction notes

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