Sodium Hydroxide → HCID 178510733, compound

Participants

Reaction Steps

Methyl cis-2-isocyanato-2-(3-methoxycarbonyl cyclobutyl)-3-(9-anthracenyl)propanoate (65 mg, 0.16 mmol) was treated with aqueous sodium hydroxide and the reaction worked up following the procedure described in Example 16 (vi) to give the title compound as a pale yellow solid (m.p. 213-216° C.), 1H NMR (D2 0/NaOD) δ 8.42(s), 8.35(d), 8.06(s), 8.02(d),7.50-7.58 (m), 3.87 (dd), 2.70-2.92 (m), 1.88-2.06(m)

Provenance & Evidence