Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium borohydride → HCID 18791153, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 반응물 | 9H-Thioxanthen-9-one, 1-chloro-4-propoxy- | HCID 5212856 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 18791153 | HCID 18791153 | — |
반응 단계
1-Chloro-4-propoxy-9H-thioxanthen-9-one (20 g, 65.6 mmol) was reduced with sodium borohydride (6.5 g, 0.17 mol) in methanol (320 ml) and worked up following the procedure described in Example 22(i) to give the title compound as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06054448 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-90f7ade9f8324d909462b3bb2ca3511b |
| 출처 메모 | uspto-grants-2000_04 |